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LGD-4033/MK-2866 Ingredient Identification, Purity, and Concentration. / R29644

Prepared for:
Olympus Labs UK 
www.olympuslabs.uk
April 16, 2023 

Client & Sample Information

Client: Olympus Labs UK
www.olympuslabs.uk
Study: 
LGD-4033/MK-2866 Ingredient Identification, Purity, and Concentration
Task Number: #29644
Batch Number: OL2212
Verification Key: TST4ESLRXE85 – Verify

Summary

Raw Material: MK-2866 | Molecular Formula: C19H14F3N3O3 | Molecular Weight: 389.33 CAS No.: 841205-47-8

Raw Material: LGD-4033 | Molecular Formula: C14H12F6N2O | Molecular Weight: 338.25 CAS No.: 1165910-22-4

Purity:

The raw material of LGD-4033/MK-2866 powder was tested by HPLC-MS for purity.  Based on the HPLC chromatographic purity measurement, the raw materials of LGD-4033 & MK-2866 were calculated to both be > 99% pure using the area normalization method.

Concentration:

A bottle labeled “LGD-4033/MK-2866” with the batch number “OL2212” was received on 14 April 2023. The powder inside the capsule was assayed for the concentrations of the intended active ingredients using HPLC-DAD. The total concentration of LGD-4033 found was 8.68mg and the total concentration of MK-2866 found was 7.94mg.

Purity:

A bottle labeled “LGD-4033/MK-2866” with the batch number “OL2212” was received on 14 April 2023. Analysis was conducted on the contents of the capsule by extraction of the active compound using GC-MS under a blind screening method developed to detect common anabolic steroids and aromatase inhibitors by Janoshik. LGD-4033 & MK-2866 were both positively identified.

Raw Material Purity Test Results

Raw Material Identification & Concentration Test Results

Results & Discussion

Bottle labeled LGD-4033/MK-2866 with batch number OL2212 was positively identified for LGD-4033 & MK-2866 with a concentration of 7.94mg per capsule of MK-2866 and 8.68mg of LGD-4033 per capsule,  with an assay of > 99% purity for each compound.

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